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Preparation and characterization of carboxymethylated gum from pilliostigama reticulatum seeds gum

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dc.contributor.author Ali, Khawla Abd Elwahab Elawad
dc.contributor.author Supervisor, -Essa Esmail Mohammad Ahmad
dc.date.accessioned 2021-05-23T13:58:39Z
dc.date.available 2021-05-23T13:58:39Z
dc.date.issued 2019-12-01
dc.identifier.citation Ali,Khawla Abd Elwahab Elawad.Preparation and characterization of carboxymethylated gum from pilliostigama reticulatum seeds gum/Khawla Abd Elwahab Elawad Ali;Essa Esmail Mohammad Ahmad.-khartoum:Sudan University Of Science & Technology,College Of Science, 2019.-143p:ill ;28cm.-Msc. en_US
dc.identifier.uri http://repository.sustech.edu/handle/123456789/26156
dc.description Thesis en_US
dc.description.abstract Carboxymethylated Piliostigama reticulatum seed gum (CM-PRSG) was prepared by treating the PRSG seed gum with monochloroacetic acid (MCA) in the presence of sodium hydroxide (NaOH). Various reaction conditions were optimized. The influence of the reaction temperatures and times, concentrations of sodium hydroxide and MCA on the degree of substitution (DS) were investigated. The result shows that Optimum preparation conditions for a CM-PRSG with DS of 0.0453 are: reaction temperature, 35оC; reaction time, 30 min; NaOH concentration was 4.15 mmol and MCA concentration was 4.15 mmol. The yield was 6.5 grams. Fourier-transform infrared analysis of the products indicates the successful carboxymethylation by the presence of the characteristics absorption bands at 1741 and 1000-1100 cm-1. en_US
dc.description.sponsorship Sudan University Of Science & Technology en_US
dc.language.iso en_US en_US
dc.publisher Sudan University Of Science & Technology en_US
dc.subject carboxymethylated en_US
dc.subject Preparation and characterization en_US
dc.title Preparation and characterization of carboxymethylated gum from pilliostigama reticulatum seeds gum en_US
dc.type Thesis en_US


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